Effect of Salt Bath and Oil Quenching Heat Treatments on SKT4 Forging Dies for Sustainable Undercarriage Link Production

Authors

DOI:

https://doi.org/10.26877/asset.v8i3.2959

Keywords:

Dies Forging, Heat Treatment, Salt Bath, SKT4, Oil Quench

Abstract

SKT4 steel, classified by the Japan Industrial Standard (JIS) as a hot-forming mold steel, is widely used for forging dies due to its favorable chemical composition and mechanical properties. During forging, dies are subjected to repeated impacts and high temperatures, which gradually reduce their performance and contribute to product defects. However, quantitative comparisons between salt bath and oil quenching treatments for SKT4 dies in high-cycle forging applications remain limited. This study evaluates the effects of salt bath and oil quenching, combined with tempering at 400°C and 450°C, on the microstructure, mechanical properties, and service performance of SKT4 dies used in undercarriage link forging. Forging trials were conducted for 3,000 and 6,000 production cycles. The results demonstrate that salt bath quenching significantly improves die hardness and wear resistance compared with oil quenching. The optimum condition was achieved with salt bath quenching followed by tempering at 400°C, producing the highest hardness of 46.1 HRC and the lowest specific wear rate of 6.98 × 10⁻⁵ mm³/kg·m. Dies treated under this condition showed no visible product defects after 6,000 forging cycles. Microstructural analysis revealed finer and more homogeneous tempered martensite laths in salt bath-quenched specimens. Unlike oil quenching, salt bath quenching eliminates vapor blanket formation, enabling direct convective cooling, more uniform temperature reduction, and minimal distortion. These findings indicate that salt bath quenching with 400°C tempering provides the optimal combination of hardness, wear resistance, and durability, supporting longer die life, reduced rework, and more sustainable forging operations.

Author Biographies

  • Wikan Jatimurti, Institut Tekonologi Sepuluh Nopember

    Departemen Teknik Material dan Metalurgi, Fakultas Teknologi Industri dan Rekayasa Sistem, Institut Tekonologi Sepuluh Nopember, Surabaya, Indonesia.

  • Muhammad Zhafran Muhadzdzib, Institut Tekonologi Sepuluh Nopember

    Departemen Teknik Material dan Metalurgi, Fakultas Teknologi Industri dan Rekayasa Sistem, Institut Tekonologi Sepuluh Nopember, Surabaya, Indonesia.

  • Agung Purniawan, Institut Tekonologi Sepuluh Nopember

    Departemen Teknik Material dan Metalurgi, Fakultas Teknologi Industri dan Rekayasa Sistem, Institut Tekonologi Sepuluh Nopember, Surabaya, Indonesia.

  • Sutarsis, Institut Tekonologi Sepuluh Nopember

    Departemen Teknik Material dan Metalurgi, Fakultas Teknologi Industri dan Rekayasa Sistem, Institut Tekonologi Sepuluh Nopember, Surabaya, Indonesia.

  • Alvian Toto Wibisono, Institut Tekonologi Sepuluh Nopember

    Departemen Teknik Material dan Metalurgi, Fakultas Teknologi Industri dan Rekayasa Sistem, Institut Tekonologi Sepuluh Nopember, Surabaya, Indonesia.

References

[1] Sakimoto, S. (2018). Advanced Manufacturing in Heavy Equipment Industry. Springer. https://doi.org/10.1007/978-3-319-68468-6.

[2] International, A. S. M. (2006). Handbook of Materials for Engineering. ASM International.

[3] Davis, J. R. (1995). Metals Handbook: Desk Edition. ASM International Handbook Committee. ISBN 0-87170-654-7.

[4] Liscic, B, dkk. (2010). Quenching Theory and Technology (2nd ed.). CRC Press. https://doi.org/10.1201/9781420009163.

[5] Totten, G. E. (2006). Steel Heat Treatment: Metallurgy and Technologies. CRC Press. Taylor & Francis Group. ISBN-13: 978-0-8493-8455-4.

[6] Grum, J. (2002). Saltbath Heat Treatment: A Practical Approach. Journal of Heat Treating, 18(4), 45–53. https://doi.org/10.1007/s11665-002-0045-8.

[7] Chander, S., & Chawla, V. (2017). Failure of Hot Forging Dies-An Updated Perspective. In Materials Today: Proceedings (Vol. 4). Ferozepur College of Engg. &Technology, Ferozepur(Punjab)-142052.

[8] Rassizadehghani, J., Raygan, S., & Askari, M. (2006). HEAT TREATMENT COMPARISON OF THE QUENCHING CAPACITIES OF HOT SALT AND OIL BATHS. In Termicheskaya Obrabotka Metallov (Issue 5.

[9] Barrena‐rodríguez, M. de J., Acosta‐gonzález, F. A., & Téllez‐rosas, M. M. (2021). A review of the boiling curve with reference to steel quenching. Metals, 11(6). https://doi.org/10.3390/met11060974

[10] Wei, M. X., Wang, S. Q., Wang, L., Cui, X. H., & Chen, K. M. (2011). Effect of tempering conditions on wear resistance in various wear mechanisms of H13 steel. Tribology International, 44(7–8), 898–905. https://doi.org/10.1016/j.triboint.2011.03.005.

[11] Cui, X. H., Wang, S. Q., Wei, M. X., & Yang, Z. R. (2011). Wear characteristics and mechanisms of h13 steel with various tempered structures. Journal of Materials Engineering and Performance, 20(6), 1055–1062. https://doi.org/10.1007/s11665-010-9723-0.

[12] Callister, W. D., & Rethwisch, D. G. (2018). Materials Science and Engineering: An Introduction (10th ed.). John Wiley & Sons.

[13] Dwi Haryadi, G. (2006). PENGARUH SUHU TEMPERING TERHADAP KEKERASAN, KEKUATAN TARIK DAN STRUKTUR MIKRO PADA BAJA K-460.

[14] Raygan, S., Rassizadehghani, J., & Askari, M. (2009). Comparison of Microstructure and Surface Properties of AISI 1045 Steel after Quenching in Hot Alkaline Salt Bath and Oil. Journal of Materials Engineering and Performance, 18(2), 168–173. https://doi.org/10.1007/s11665-008-9273

[15] Torkamani, H., Raygan, S., & Rassizadehghani, J. (2014). Comparing microstructure and mechanical properties of AISI D2 steel after bright hardening and oil quenching. Materials & Design, 54, 1049–1055. https://doi.org/10.1016/j.matdes.2013.09.043 (Perbandingan langsung salt bath alkaline vs oil quenching pada tool steel — sangat relevan untuk pembahasan mikrostruktur dan sifat mekanik.)

[16] Gronostajski, Z., Kaszuba, M., Polak, S., Zwierzchowski, M., Niechajowicz, A., & Hawryluk, M. (2016). The failure mechanisms of hot forging dies. Materials Science and Engineering: A, 657, 147–160. https://doi.org/10.1016/j.msea.2016.01.030

[17] Ghalehbandi, S. M., & Biglari, F. (2020). Predicting damage and failure under thermomechanical fatigue in hot forging tools. Engineering Failure Analysis, 113, 104545. https://doi.org/10.1016/j.engfailanal.2020.104545

[18] Hawryluk, M., Ziemba, J., Dworzak, Ł., Kaczyński, P., & Kasprzak, M. (2018). Wear analysis of forging tools used in the hot forging processes using 3D reverse scanning techniques and cooling-lubricating system. The International Journal of Advanced Manufacturing Technology, 97(5–8), 2185–2196. https://doi.org/10.1007/s00170-018-2066-y

[19] Abd AL-Kareem Ahmed, I., Mohammed, A., & Allow, M. (2021). Improvement of forging die life by failure mechanism analysis. Journal of the Mechanical Behavior of Materials, 30(1), 309–317. https://doi.org/10.1515/jmbm-2021-0034

[20] Lisiecki, Ł., & Bembenek, M. (2023). Tool wear issues in hot forging of steel. Materials, 16(2), 471. https://doi.org/10.3390/ma16020471

[21] Ficak, G., Łukaszek-Sołek, A., & Hawryluk, M. (2024). Durability of forging tools used in the hot closed die forging process—A review. Materials, 17(22), 5407. https://doi.org/10.3390/ma17225407

[22] Calvo-García, E., Valverde-Pérez, S., Riveiro, A., Álvarez, D., Román, M., Magdalena, C., Badaoui, A., Moreira, P., & Comesaña, R. (2022). An experimental analysis of the high-cycle fatigue fracture of H13 hot forging tool steels. Materials, 15(21), 7411. https://doi.org/10.3390/ma15217411

[23] Scharf, S., et al. (2020). Unlocking sustainability potentials in heat treatment processes. Sustainability, 12(16), 6457. https://doi.org/10.3390/su12166457 (Relevan untuk aspek "sustainable" pada judul — efisiensi energi dan pengurangan emisi pada proses heat treatment industri.)

[24] A study on factors affecting the wear of steel track undercarriage. (2023). Journal of Quality in Maintenance Engineering, 29(3), 622–639. Emerald Publishing. https://doi.org/10.1108/JQME-01-2022-0004 (Langsung relevan dengan konteks "undercarriage link production" pada judul penelitian Anda.)

[25] Rassizadehghani, J., Raygan, S., Torkamany, H., & Emamy, M. (2011). The influence of alkaline salt bath quenching on the microstructure and mechanical properties of AISI D2 steel. Journal of Materials Engineering and Performance, 20, 1057–1063. https://doi.org/10.1007/s11665-010-9754-6

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2026-07-28

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